Michael M. Woolfson's An Introduction to X-ray Crystallography, Second Edition PDF

By Michael M. Woolfson

ISBN-10: 0511622554

ISBN-13: 9780511622557

ISBN-10: 0521412714

ISBN-13: 9780521412711

ISBN-10: 0521423597

ISBN-13: 9780521423595

A textbook for the senior undergraduate or graduate pupil starting a significant examine of X-ray crystallography. will probably be of curiosity either to these aspiring to turn into expert crystallographers and to these physicists, chemists, biologists, geologists, metallurgists and others who will use it as a device of their examine. All significant points of crystallography are covered--the geometry of crystals and their symmetry, theoretical and useful facets of diffracting X-rays through crystals and the way the information will be analyzed to discover the symmetry of the crystal and its constitution. contains contemporary advances equivalent to the synchrotron as a resource of X-rays, equipment of fixing buildings from strength information and the complete variety of concepts for fixing buildings from single-crystal information. computing device courses are supplied for conducting many operations of data-processing and fixing crystal buildings together with by way of direct equipment. those courses are required for lots of of the examples given on the finish of every bankruptcy yet can be utilized to create new examples wherein scholars can try out themselves or one another.

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Extra info for An Introduction to X-ray Crystallography, Second Edition

Sample text

Ill of the International Tables for X-ray Crystallography. Various models of atoms have been used to give electron-density distributions. For light atoms the Hartree self-consistent field method of computing wave functions is usually employed, while for heavy atoms the Thomas-Fermi approximation may be used. We can now investigate the nature of Compton scattering from atoms. 36) we can see that the intensity of coherent scattering from an atomic electron is p\^ 2Q and hence, since the total intensity of scattering as revealed by wave mechanics is J2By the intensity of the Compton scattering must be (1 — Ps)^2o- However the Compton scattering from one atomic electron is incoherent with respect to that scattered by any other and hence the total intensity from all the electrons is obtained by adding the individual intensities from each of the electrons.

28 and shows the fourfold axes, two sets of glide lines at an angle TI/4 to each other and a set of mirror lines at n/4 to the edges of the cell. Starting with a single structural unit there are generated seven others; the resultant eight structural units are the contents of the square cell. Wherever a pair of structural units are related by either a mirror line or a glide line the enantiomorphic relationship is shown by the presence of a comma in one of them. Fig. 28. The two-dimensional space group p4g as it appears in International Tables for X-ray Crystallography.

Rotation axes (2, 3, 4, 6) The modes of operation of rotation axes are shown in fig. 7; the new feature which arises for a repeated pattern is the generation of subsidiary axes of symmetry other than those put in initially. This may be seen in fig. 25(d) which shows a projected view of a tetragonal unit cell down the tetrad axis. The point Ax is operated on by the tetrad axis through O to give A2, A3 and A± and this pattern is repeated about every equivalent tetrad axis. It is clear that Al9 A'2, A^ and A'£ are related by a tetrad axis, non-equivalent to the one through 0, through the centre of the cell.

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An Introduction to X-ray Crystallography, Second Edition by Michael M. Woolfson


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